- Research on Synthesis and Sintering Behavior of Nano-sized (Pb, La)TiO3 Powders Using Mechano Chemical Process
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Young-In Lee, Yong-Sung Goo, Jong-Sik Lee, Yong-Ho Choa
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J Korean Powder Metall Inst. 2010;17(2):101-106.
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DOI: https://doi.org/10.4150/KPMI.2010.17.2.101
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 Abstract
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- In this study, we successfully synthesized a nano-sized lanthanum-modified lead-titanate (PLT) powder with a perovskite structure using a high-energy mechanochemical process (MCP). In addition, the sintering behavior of synthesized PLT nanopowder was investigated and the sintering temperature that can make the full dense PLT specimen decreased to below 1050°C by using Bi_2O_3 powder as sintering agent. The pure PLT phase of perovskite structure was formed after MCP was conducted for 4 h and the average size of the particles was approximately 20 nm. After sintered at 1050 and 1150°C, the relative density of PLT was about 93.84 and 95.78%, respectively. The density of PLT increased with adding Bi_2O_3 and the specimen with the relative densitiy over 96% were fabricated below 1050°C when 2 wt% of Bi_2O_3 was added.
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